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1 article(s) from Tanner, Susanne

Synthesis and crossover reaction of TEMPO containing block copolymer via ROMP

Olubummo Adekunle,
Susanne Tanner and
Wolfgang H. Binder

Beilstein J. Org. Chem. 2010, 6, No. 59, doi:10.3762/bjoc.6.59

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Graphical Abstract

Scheme 1: Grubbs G1–G3 and Umicore U1–U3 catalyst.

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Scheme 2: Synthetic pathway to BCP-A_nT_m using Grubbs’ (1–3) and Umicore (4–6) type catalysts.

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Figure 1: ¹H NMR spectrum of the homopolymer A₅₀ synthesized with the catalyst U3.

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Figure 2: ¹³C NMR spectrum of the homopolymer A₅₀ synthesized with catalyst U3.

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Figure 3: Kinetic progress monitored via ¹H NMR spectroscopy of the polymerization of monomer A 7 with cataly...

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Figure 4: Kinetic progress monitored via ¹H NMR spectroscopy of the polymerization of 7 with catalyst U3; [7]...

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Figure 5: ln([M]₀/[M]_t) vs. time (t) plot obtained from ¹H NMR spectra for homopolymer-A₅₀ using catalyst U3;...

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Figure 6: M_n vs. time (t) kinetic plot and M_w/M_n (PDI) of the polymerization of monomer T 9 with catalyst U3;...

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Figure 7: GPC trace of the block copolymer A₂₅T₂₅ synthesized with catalyst U3.

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Figure 8: MALDI-TOF mass spectra of homopolymer A₂₅ 4 synthesized with catalyst U3: (a) full spectrum, (b) ex...

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Figure 9: MALDI-TOF mass spectrum of BCP-A₂₅T₁ synthesized with catalyst U3.

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Figure 10: MALDI-TOF mass spectrum of BCP-A₂₅T₂ 13 synthesized with catalyst U3.

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Figure 11: MALDI-TOF mass spectrum of BCP-A₂₅T₂₅ synthesized with catalyst U3.

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Published 01 Jun 2010

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